Calculate the volume of NaOH required for each of the other three samples and titrate them carefully. During each titration, periodically tilt and rotate the flask to wash liquid from the walls into the solution. When very near the end, deliver less than 1 drop of titrant at a time. To do this, carefully suspend a fraction of a drop from the buret tip, touch it to the inside wall of the flask, wash it into the bulk solution by careful tilting, and swirl the solution. The end point is the first appearance of pink color that persists for 15 s. The color will slowly fade as CO from air dissolves in the solution.
Calculate the volume of NaOH required for each of the other …
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